安捷倫1260II高效液相色譜儀
1儀器介紹
Agilent 1260 Infinity II 液相色譜系統(tǒng) 與新色譜柱技術(shù)和先進(jìn)的備件相結(jié)合,可保證穩(wěn)定可靠的分離和檢測性能。1260 Infinity II 四元泵能夠提供達(dá) 600 bar 的壓力,完美適用于InfinityLab Poroshell 120 色譜柱。無脈沖、穩(wěn)定而混合均勻的梯度可確保獲得更的靈敏度和更可靠的結(jié)果,而較小的填料顆?蓪崿F(xiàn)更快速的分離和更的分離度。這款泵多支持四種溶劑,使您在自動溶劑混合中獲得極靈活性,適用于各種研究和常規(guī)應(yīng)用。穩(wěn)定的材料能夠耐受苛刻的應(yīng)用,能夠支持泵持續(xù)運行數(shù)年,從而大程度縮短停機時間并降低運行成本。 在分析生物樣品或需要采用極端 pH 條件的應(yīng)用中,可采用度耐腐蝕的鈦金屬四元泵。與其他 1260 Infinity II 生物惰性模塊結(jié)合后,即可配置出安捷倫獨有的包含完全無金屬樣品流路、且壓力范圍達(dá) 600 bar 的系統(tǒng)。 1260 Infinity II 容量柱溫箱多可容納四根 30 cm 色譜柱,并可通過 InfinityLab 快速更換切換閥直接操作每根色譜柱。無需斷開并重新連接色譜柱即可自動運行不同方法。全部四根色譜柱均包含的固定式標(biāo)簽可記錄色譜柱 ID 和完整使用歷史,確保符合法規(guī)指南要求。色譜柱追蹤也有助于避免重要序列運行過程中的故障,或避免固定相、溶劑和溫度不匹配。 二極管陣列檢測器的靈敏度流通池能夠檢測極低的樣品濃度。我們還為二極管陣列檢測器和熒光檢測器提供了殊的生物惰性流通池,確保對生物樣品實現(xiàn)安全的數(shù)據(jù)采集。
2指標(biāo)
Physical Specifications Agilent 1260 Infinity II Isocratic Pump(G7110B)
安捷倫1260ⅡG7110B等度泵
Physical Specifications Agilent 1260 Infinity II Quaternary Pump VL
(G7111A)
Table 2 Physical Specifications
Physical Specifications Agilent 1260 Infinity II Quaternary Pump
(G7111B)
Table 3 Physical Specifications
Physical Specifications Agilent 1260 Infinity II -G7102A Physical Specifications
Performance Specification of the ELS Detector
G7114B Physical Specifications
Agilent 1260 Infinity II Variable Wavelength Detector (G7114A) Performance Specifications
Physical Specifications G7115A
Performance Specifications G7115A
Agilent 1260 Infinity II Variable Wavelength Detector (G7116A) Physical Specifications
Agilent 1260 Infinity II Multicolumn Thermostat (G7116A) Performance Specifications
Agilent 1260 Infinity II Variable Wavelength Detector (G7117A) Physical Specifications
Agilent 1260 Infinity II Variable Wavelength Detector (G7117A) Performance Specifications
Agilent 1290 Infinity II Diode Array Detector (G7117B) Performance Specifications
Agilent 1290 Infinity II High Speed Pump (G7120A) Physical Specifications
Agilent 1290 Infinity II High Speed Pump (G7120A) Performance Specifications
Agilent 1290 Infinity II High Speed Pump (G7120A) Performance Specifications
G7121A Physical Specifications
Performance Specifications Agilent 1260 Infinity II Fluorescence Detector
SPECTRA (G7121B)
G7129AB Physical Specifications
Performance Specifications (G7129A)
Performance Specifications (G7129B)
Physical Specifications (G7162A)
Physical Specifications Agilent 1260 Infinity II Multisampler
(G7167B)
Physical Specifications Agilent 1260 Infinity II Bio-inert
Multisampler (G5668A)
Table 3 Agilent 1290 Infinity II Multisampler (G7167B) Performance Specifications
Performance Specifications (G7167A)
Table 4 Agilent 1260 Infinity Multisampler (G7167A) Performance Specifications
P
Performance Specifications G5668A
Table 5 Agilent 1260 Infinity II Bio-inert Multisampler (G5668A) Performance Specifications
Physical Specifications of the Sample Cooler
Table 6 Physical Specification of the Sample Cooler
Table 7 Performance Specifications Agilent 1290 Sample Cooler
安捷倫1260ⅡG7110B等度泵
Type | Specification | Comments |
Weight | 14.7 kg (32 lbs) | |
Dimensions (height × width × depth) | 180 x 396 x 436 mm (7.1 x 15.6 x 17.2 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 80 VA, 65 W | |
Ambient operating temperature | 4–55 °C (39–131 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
(G7111A)
Table 2 Physical Specifications
Type | Specification | Comments |
Weight | 14.7 kg (32 lbs) | |
Dimensions (height × width × depth | 180 x 396 x 436 mm (7.1 x 15.6 x 17.2 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 80 VA, 65 W | |
Ambient operating temperature | 4–55 °C (39–131 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
Type | Specification | Comments |
Weight | 14.7 kg (32 lbs) | |
Dimensions (height × width × depth | 180 x 396 x 436 mm (7.1 x 15.6 x 17.2 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 80 VA, 65 W | |
Ambient operating temperature | 4–55 °C (39–131 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
(G7111B)
Table 3 Physical Specifications
Type | Specification | Comments |
Weight | 14.7 kg (32 lbs) | |
Dimensions (height × width × depth) | 180 x 396 x 436 mm (7.1 x 15.6 x 17.2 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 80 VA, 65 W | |
Ambient operating temperature | 4–55 °C (39–131 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
Type | Specification | Comments |
Weight | 11 kg (non-cooled), 13 kg (cooled) | |
Dimensions (height × width × depth) |
415 x 200 x 450 mm (16.3 x 7.9 x 17.7 inches) |
|
Line voltage | 100 – 240 V~, ± 10 % |
Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 150 W (max) | Maximum |
Ambient operating temperature |
10–35 °C (50–95 °F) | |
Ambient non-operating temperature |
-40 – 70 °C (-40 – 158 °F) | |
Humidity | < 80 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 2000 m (6562 ft) | |
Non-operating altitude | Up to 4600 m (15091 ft) | For storing the module |
Safety standards: IEC, CSA, UL |
Installation category II, Pollution degree 2 | For indoor use only. |
Type | Specification |
Light Source | |
G7102A | LASER 405 nm, 10 mW (Class 3B) |
Detector | Dual PMT with digital signal processing |
Nebuliser | OFF, 25 – 90 °C |
Evaporator | |
Non-cooled | OFF, 25 – 120 °C |
Cooled | OFF, 10 – 80 °C |
Gas Flow Range | 0.9 – 3.25 SLM (controlled gas shut-off) |
Short Term Noise | <0.1 mV under specified condtions. See “Specification Conditions” on page 24. |
Drift | <1 mV/h under specified condtions. See “Specification Conditions” on page 24. |
Operating Pressure | 60 – 100 psi (4.1 – 6.9 bar) |
Eluent Flow range | 0.2 – 5.0 mL/min |
Digital Output | 10, 40 or 80 Hz (24 bit) |
Type | Specification | Comments |
Weight | 11 kg (24.3 lbs) | |
Dimensions (height × width × depth) | 140 x 396 x 436 mm (5.5 x 15.6 x 17.2 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 80 VA, 70 W | |
Ambient operating temperature | 4 - 55 °C (39 - 131 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
Feature | Specification |
Detection type | Double-beam photometer |
Light source | Deuterium lamp |
Number of signals | Single and dual wavelength detection |
Maximum data rate | 120 Hz (single wavelength detection) 2.5 Hz (dual wavelength detection) |
Noise | <±0.25·10-5 AU, at 230 nm (single wavelength detection) <±0.80·10-5 AU, at 230 nm and 254 nm (dual wavelength detection) |
Drift | <1·10-4 AU/h, at 230 nm |
Linearity | >2.5 AU upper limit |
Wavelength range | 190 – 600 nm |
Wavelength accuracy | ±1 nm, self-calibration with deuterium lines, verification with holmium oxide filter |
Wavelength precision | <±0.1 nm |
Slit width | 6.5 nm typical over whole wavelength range |
Time programmable | Wavelength, polarity, peak width, lamp on/off |
Flow cells | Standard: 14 μL volume, 10 mm cell path length and 40 bar (588 psi) pressure maximum Micro: 2 μL volume, 3 mm cell path length and 120 bar (1760 psi) pressure maximum Semi-micro: 5 μL volume, 6 mm cell path length and 40 bar (588 psi) pressure maximum Preparative: 4 μL volume, 3 mm cell path length and 120 bar (1760 psi) pressure maximum Preparative: 0.3 mm cell path length and 50 bar (725 psi) pressure maximum Preparative: 0.06 mm cell path length and 50 bar (725 psi) pressure maximum High pressure: 14 μL volume, 10 mm cell path length and 400 bar (5801 psi) pressure maximum |
Spectral tools | Stop-flow wavelength scan |
Analog output | Recorder/Integrator 100 mV or 1 V, 1 output |
Communication | LAN, Controller-area network (CAN), ERI: ready, start, stop and shut-down signals, USB |
GLP | Early maintenance feedback (EMF) for continuous tracking of instrument usage in terms of lamp burn time with user settable limits and feedback messages. Electronic records of maintenance and errors. RFID for electronics records of flow cell and UV lamp conditions (path length, volume, product number, serial number, test passed, and usage). Verification of wavelength accuracy with built-in holmium oxide filter. |
Safety and maintenance | Extensive diagnostics, error detection and display through Agilent Instant Pilot and Agilent Lab Advisor software. Leak detection, safe leak handling, leak output signal for shutdown of pumping system. Low voltages in major maintenance areas. Tracking of flow cells and lamps with RFID (radio frequency identification) tags |
Type | Specification | Comments |
Weight | 12 kg (26.5 lbs) | |
Dimensions (height × width × depth) | 140 x 396 x 436 mm (5.5 x 15.6 x 17 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 110 VA / 100 W | |
Ambient operating temperature | 4–55 °C (39–131 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
Type | Specification | Comments |
Detection type | 1024-element photodiode array | |
Light source | Deuterium and tungsten lamps | The UV-lamp is equipped with RFID tag that holds lamp typical information. |
Data rate | up to 120 Hz | |
Wavelength range | 190 – 950 nm | |
Short term noise (ASTM) Single and Multi-Wavelength | < ± 0.7·10-5 AU at 254 and 750 nm | see "Specification Conditions" below |
Drift | < 0.9·10-3 AU/h at 254 nm | see "Specification Conditions" below |
Linear absorbance range | > 2 AU (5 %) at 265 nm | see "Specification Conditions" below |
Wavelength accuracy |
± 1 nm |
Self-calibration with deuterium lines, verification with holmium oxide filter |
Wavelength bunching | 1 – 400 nm | Programmable in steps of 1 nm |
Slit width | 1, 2, 4 , 8, 16 nm | Programmable slit |
Diode width | < 1 nm | |
Flow cells | Standard: 13 μL volume, 10 mm cell path length and 120 bar (1740 psi) pressure maximum Standard bio-inert: 13 μL volume, 10 mm cell path length and 120 bar (1740 psi) pressure maximum Semi-micro: 5 μL volume, 6 mm cell path length and 120 bar (1740 psi) pressure maximum Micro: 2 μL volume, 3 mm cell path length, 120 bar (1740 psi) pressure maximum Semi-nano: 500 nL volume, 10 mm cell path length and 50 bar (725 psi) pressure maximum Nano: 80 nL volume, 6 mm cell path length and 50 bar (725 psi) pressure maximum High pressure: 1.7 μL volume, 6 mm cell path length and 400 bar (5800 psi) pressure maximum Prep SST: 3 mm cell path length and 120 bar (1740 psi) pressure maximum Prep Quartz:0.3 mm cell path length and 20 bar (290 psi) pressure maximum Prep Quartz: 0.06 mm cell path length and 20 bar (290 psi) pressure maximum | All flow cells are equipped with RFID tags that hold cell typical information. pH range 1.0 – 9.5 (12.5 solvent dependent with bio-inert version |
Time programmable | Wavelength, polarity, peak width, lamp bandwidth, autobalance, wavelength range, threshold, spectra storage mode | |
Spectral tools | Data analysis software for spectra evaluation, including spectral libraries and peak purity functions | |
Control and data evaluation | Agilent OpenLab CDS |
• OpenLab CS C.01.07 • Driver A.02.14 |
Type | Specification | Comments |
Weight | 12.5 kg (27.6 lbs) | |
Dimensions (height × width × depth) | 160 x 435 (472*) x 436 mm (6.3 x 17.1 (18.6*) x 17.2 inches) *with column ID kit | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 150 VA, 150 W | |
Ambient operating temperature | 4–55 °C (39–131 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
Feature | Specification1 |
Operating principle | Thermostatted column compartment with dual, independent Peltier-element. Solvent pre-heating and still-air operation for reduction of chromatographic band-broadening under UHPLC-conditions. |
Temperature range | 10 °C below ambient (minimum 4 °C) to 85 °C settable in steps of 0.1 K |
Temperature stability | ±0.1 °C |
Temperature accuracy | ±0.5 °C (with calibration for 40 °C) |
Temperature precision | 0.05 °C |
Independent Temperature zones | 2in single device |
Column capacity | 4 columns of up to 300 mm length plus A-Line Quick-Connect fittings or pre-column Number of pre column Quick-Connect Heat Exchangers is scalable – each column can be equipped with individual heat exchanger for best performance 4-column selector valve is available to access each column without replumbing |
Heat-up/cool-down time | 5 min from ambient to 40 °C 10 min from 40 °C to 20 °C <25 min from 25 °C to 85 °C |
Solvent heat exchangers | For pre-column solvent heating, G7116A is equipped with a Quick-Connect Heat Exchanger Large ID (0.17 mm capillary, 3 μL internal volume) as default. Other dimensions of Quick-Connect Heat Exchangers are optionally available as well as heat exchangers made out of bio-inert materials (metal-free). |
Valve options | 1 x integrated valve drive as option to host user-exchangeable Quick-Change valve heads (up to 600 bar) of different formats: 2-position/6-port, 2-position/10-port, 4-column selection. Also available in bio-inert materials. Valve heads are automatically identified by their tag. |
Column identification | Optionally, column identification kit to track history of up to four columns. Mounted left hand-side of module. |
Communications | Controller-area network (CAN). G7116A is a hosted module (LC stack needs to contain a LAN communication and control card) |
Software compatibility | Requires OpenLAB CDS A.01.03 - A.02.02 (with LC & CE Drivers A.02.14) ?昈penLAB CDS ChemStation ed. C.01.03 -C.01.07 SR2 or higher ?OpenLAB CDS EZChrom ed. A.04.05 - A.04.07 SR2 or higher MassHunter (LC Drivers A.02.14) ?MassHunter B.07.01 or higher for (Q)-TOF ?MassHunter B.08.02 or higher for QQQ |
Safety and maintenance | Extensive diagnostics, error detection and display (through Instant Pilot control module and Agilent LabAdvisor), leak detection, safe leak handling, leak output signal for shutdown of pumping system. Low voltages in main maintenance areas. |
GLP | Valve heads carrying tags with serial number, pressure rating, number of switches and valve type. Concept of column identification. |
Type | Specification | Comments |
Weight | 11.5 kg (25.4 lbs) | |
Dimensions (height × width × depth) | 140 x 396 x 436 mm (5.5 x 15.6 x 17.2 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 110 VA, 100 W | |
Ambient operating temperature | 4 – 40 °C (39 – 104 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
Feature | Specification |
Detector type | 1024-element diode array |
Light source | Deuterium |
Number of signals | 8 |
Maximum sampling rate | 120 Hz (both spectra and signals) |
Short-term noise | with 10 mm Max-Light cartridge cell: <±3·10-6 AU at 230/4 nm, slit width 4 nm, TC 2 s, ASTM with 60 mm Max-Light cartridge cell: <±0.6·10-6 AU/cm at 230/4 nm, slit width 4 nm, TC 2 s, ASTM |
Drift | <0.5·10-3 AU/h at 230 nm |
Linearity | >2.0 AU (5 %) at 265 nm Typically 2.5 AU (5 %) |
Wavelength range | 190 – 640 nm |
Wavelength accuracy | ±1 nm, self-calibration with deuterium lines |
Wavelength precision | <±0.1 nm |
Diode width | ~0.5 nm |
Wavelength bunching | Programmable, 2 – 400 nm, in steps of 1 nm |
Flow cells | User-exchangeable, self-aligning cartridge cells with RFID tags. Max-Light Cartridge Cell (Standard): 10 mm, σV = 1.0 μL Max-Light Cartridge Cell (High Sensitivity): 60 mm, σV = 4 μL Max-Light Cartridge Ultra Low Dispersion (ULD) Cell: 10 mm, σV = 0.6 μL Max-Light Cartridge High Dynamic Range (HDR) Cell: 3.7 mm, σV = 0.8 μL Maximum Operating Pressure (MOP)1: 70 bar Maximum Incidental Pressure (MIP)2: 150 bar |
Spectral tools | Data analysis software for spectra evaluation, including spectral libraries and peak purity functions |
Analog output | Recorder/integrator: 100 mV or 1 V, output range 0.001 – 2 AU, one outpu |
Communications | LAN, controller-area network (CAN), ERI: ready, start, stop and shut-down signals USB |
GLP features | RFID for electronics records of flow cell and UV lamp conditions (path length, volume, product number, serial number, test passed, usage) Early maintenance feedback (EMF) for continuous tracking of instrument usage in terms of lamp burn time with user settable limits and feedback messages. Electronic records of maintenance and errors. Verification of wavelength accuracy with deuterium lines. |
Safety and maintenance | Extensive diagnostics, error detection and display through Agilent Instant Pilot and Agilent Lab Advisor software. Leak detection, safe leak handling, leak output signal for shutdown of pumping system. Low voltages in major maintenance areas. |
Others | Second generation of Electronic temperature control (ETC) for the complete optical unit |
Feature | Specification |
Detector type | 1024-element diode array |
Light source | Deuterium |
Number of signals | 8 |
Maximum sampling rate | 240 Hz (both spectra and signals) |
Short-term noise | with 10 mm Max-Light cartridge cell: <±3·10-6 AU at 230/4 nm, slit width 4 nm, TC 2 s, ASTM with 60 mm Max-Light cartridge cell: <±0.6·10-6 AU/cm at 230/4 nm, slit width 4 nm, TC 2 s, ASTM |
Drift | <0.5·10-3 AU/h at 230 nm |
Linearity | >2.0 AU (5 %) at 265 nm Typically 2.5 AU (5 %) |
Wavelength range | 190 – 640 nm |
Wavelength accuracy | ±1 nm, self-calibration with deuterium lines |
Wavelength precision | <±0.1 nm |
Slit width | Programmable: 1, 2, 4, 8 nm |
Diode width | ~0.5 nm |
Wavelength bunching | Programmable, 2 – 400 nm, in steps of 1 nm |
Spectral tools | Data analysis software for spectra evaluation, including spectral libraries and peak purity functions |
Flow cells | User-exchangeable, self-aligning cartridge cells with RFID tags. Max-Light Cartridge Cell (Standard): 10 mm, σV = 1.0 μL Max-Light Cartridge Cell (High Sensitivity): 60 mm, σV = 4 μL Max-Light Cartridge Ultra Low Dispersion (ULD) Cell: 10 mm, σV = 0.6 μL Max-Light Cartridge High Dynamic Range (HDR) Cell: 3.7 mm, σV = 0.8 μL Maximum Operating Pressure (MOP)1: 70 bar Maximum Incidental Pressure (MIP)2: 150 bar |
Analog output | Recorder/integrator: 100 mV or 1 V, output range 0.001 – 2 AU, one output |
Communications | LAN, controller-area network (CAN), ERI: ready, start, stop and shut-down signals, USB |
GLP features | RFID for electronics records of flow cell and UV lamp conditions (path length, volume, product number, serial number, test passed, usage) Early maintenance feedback (EMF) for continuous tracking of instrument usage in terms of lamp burn time with user settable limits and feedback messages. Electronic records of maintenance and errors. Verification of wavelength accuracy with deuterium lines. |
Safety and maintenance | Extensive diagnostics, error detection and display through Agilent Instant Pilot and Agilent Lab Advisor software. Leak detection, safe leak handling, leak output signal for shutdown of pumping system. Low voltages in major maintenance areas. |
Others | Second generation of Electronic temperature control (ETC) for the complete optical unit |
Type | Specification | Comments |
Weight | 21.0 kg (46.3 lbs) | |
Dimensions (height × width × depth) | 200 x 396 x 436 mm (7.9 x 15.6 x 17.2 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 210 VA / 180 W | |
Ambient operating temperature | 4 – 55 °C (39 – 131 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
Feature | Specification |
Hydraulic system | Two dual pistons in series, pumps with proprietary servo-controlled variable stroke design and smooth motion control. |
Pump resolution step size | 300 pL step size |
Settable flow range | 0.001 – 5 mL/min, in 0.001 mL/min increments (executed in 300 pL/step increments). |
Flow precision | ≤0.07 % RSD or 0.005 min SD, whatever is greater |
Flow accuracy | ±1 % or 10 μL/min, whatever is greater |
Pressure range | up to 130 MPa (1300 bar) at 0 – 2 mL/min ramping down to 80 MPa (800 bar) at 5 mL/min |
Pressure pulsation | <1 % amplitude or <0.5 MPa (5 bar), whatever is greater |
Compressibility compensation | Automatic |
Recommended pH-range | 1.0 – 12.5, solvents with pH <2.3 should not contain acid which attack stainless steel. |
Gradient formation | High pressure binary mixing |
Delay volume | As low as 45 μL (10 μL without mixer) |
Composition precision | <0.15 % RSD or 0.01 min SD, whatever is greater |
Composition accuracy | ±0.35 % absolute |
Number of solvent | 2 out of maximum 26 solvents |
Solvent selection valve | Internal 4-solvent selection valve included. External 2x 12 solvent valve as option, fully integrated in the pump control interface. |
Feature | Specification |
Hydraulic system | Two dual pistons in series, pumps with proprietary servo-controlled variable stroke design and smooth motion control. |
Pump resolution step size | 300 pL step size |
Settable flow range | 0.001 – 5 mL/min, in 0.001 mL/min increments (executed in 300 pL/step increments). |
Flow precision | ≤0.07 % RSD or 0.005 min SD, whatever is greater |
Flow accuracy | ±1 % or 10 μL/min, whatever is greater |
Pressure range | up to 130 MPa (1300 bar) at 0 – 2 mL/min ramping down to 80 MPa (800 bar) at 5 mL/min |
Pressure pulsation | <1 % amplitude or <0.5 MPa (5 bar), whatever is greater |
Compressibility compensation | Automatic |
Recommended pH-range | 1.0 – 12.5, solvents with pH <2.3 should not contain acid which attack stainless steel. |
Gradient formation | High pressure binary mixing |
Delay volume | As low as 45 μL (10 μL without mixer) |
Composition precision | <0.15 % RSD or 0.01 min SD, whatever is greater |
Composition accuracy | ±0.35 % absolute |
Number of solvent | 2 out of maximum 26 solvents |
Solvent selection valve | Internal 4-solvent selection valve included. External 2x 12 solvent valve as option, fully integrated in the pump control interface. |
Type | Specification | |
Weight | 11.9 kg (26.2 lbs) | |
Dimensions (height × width × depth) | 140 x 396 x 436 mm (5.5 x 15.6 x 17.0 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 70 VA, 60 W | |
Ambient operating temperature | 4-55 °C (39-131 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
Type | Specification | |
Weight | 11.9 kg (26.2 lbs) | |
Dimensions (height × width × depth) | 140 x 396 x 436 mm (5.5 x 15.6 x 17.0 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 70 VA, 60 W | |
Ambient operating temperature | 4-55 °C (39-131 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
SPECTRA (G7121B)
Type | Specification | Comments |
Detection type | Multi-signal fluorescence detector with rapid on-line scanning capabilities and spectral data analysis | |
Performance specifications | Single wavelength operation: • RAMAN (H2O) > 500 (noise reference measured at signal) Ex=350 nm, Em=397 nm, dark value 450 nm, standard flow cell • RAMAN (H2O) > 3000 (noise reference measured at dark value) Ex=350 nm, Em=397 nm, dark value 450 nm, standard flow cell Dual wavelength operation: RAMAN (H2O) > 300 Ex 350 nm, Em 397 nm and Ex 350 nm, Em 450 nm, standard flow cell. | Reference conditions: Standard cell 8 μL, response time 4 s, HPLC-grade water and restriction capillary. For details refer to the Service Manual. |
Light source | Xenon Flash Lamp, normal mode 20 W, economy mode 5 W, lifetime 4000 h | |
Pulse frequency | 296 Hz for single signal mode 74 Hz for economy mode | |
Maximum data rate | 74 Hz, 148 Hz | |
Excitation monochromator | Range: settable 200 nm - 1200 nm and zero-order Bandwidth: 20 nm (fixed) Monochromator: concave holographic grating, F/1.6, blaze: 300 nm | |
Emission monochromator | Range: settable 200 nm - 1200 nm and zero-order Bandwidth: 20 nm (fixed) Monochromator: concave holographic grating, F/1.6, blaze: 400 nm | |
Reference system | in-line excitation measurement | |
Timetable programing | up to 4 signal wavelengths, response time, PMT Gain, baseline behavior (append, free, zero), spectral parameters | |
Spectrum acquisition | Excitation or Emission spectra Scan speed: 28 ms per datapoint (e.g. 0.6 s/spectrum 200 – 400 nm, 10 nm step) Step size: 1 – 20 nm Spectra storage: All | |
Wavelength characteristic | Repeatability +/- 0.2 nm Accuracy +/- 3 nm setting | |
Flow cells | Standard: 8 μL volume and 20 bar (2 MPa) pressure maximum, fused silica block Optional: • Bio-inert: 8 μL volume and 20 bar (2 MPa) pressure maximum, (pH 1–12) • Micro: 4 μL volume and 20 bar (2 MPa) pressure maximum | |
Control and data evaluation | Agilent ChemStation for LC, Agilent Instant Pilot G4208A with limited spectral data analysis and printing of spectra |
Type | Specification | Comments |
Weight | 19 kg (41.9 lbs) | w/o sample cooler |
Dimensions (height × width × depth) | 324 x 396 x 468 mm (12.8 x 15.6 x 18.4 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 350 VA / 350 W / 1195 BTU/h | |
Ambient operating temperature | 4 - 40 °C (39 - 104 °F), without chiller up to 55 °C (131 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F)1 | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
Permitted solvents | Boiling point ≥56 °C Auto-ignition temperature ≥200 °C |
Type | Specification | Comment |
Injection range | 0.1 – 100 μL in 0.1 μL increments with 100 μL up to 60 MPa 0.1 – 900 μL in 0.1 μL increments with 900 μL up to 40 MPa | Up to 1800 μL with multiple draw (hardware modification required) Requires 900 μL analytical head |
Precision | <0.25 % RSD of peak areas from <5 μL to 100 μL | Measured caffeine |
Pressure range | 0 – 60 MPa (0 – 600 bar, 0 – 8702 psi) 0 – 40 MPa (0 – 400 bar, 0 – 5801 psi) | for 900 μL Analytical Head |
Sample viscosity range | 0.2 – 5 cp | |
Sample capacity | 132 x 2 mL vial (two trays default) 100 x 2 mL vial (two classic trays optional) 36 x 6 mL vials (two trays optional) | |
Carry over | <0.004 % (40 ppm) with needle wash | Using the following conditions: • ZORBAX Eclipse Plus C18, RRHD, 2.1 x 50 mm, 1.8 μm (959757-902) • Mobile Phase: • A: 0.1 % TFA in water • B: 0.1 % TFA in acetonitrile • Isocratic : % B=33 % • Flow rate: 0.5 mL/min • Column temperature: 50 °C • Wavelength detection: 257/4 nm, ref. wavelength 380/100 nm, 20 Hz • Injection volume: 1 μL • Sample: 1200 ng/μL Chlorhexidine for UV, (dissolved with mobile phase A), 1 μL injected and measured both on Agilent G7117B DAD • Wash solution: H2O with 0.1 % TFA (5 s) |
Injection cycle time | 18 s for draw speed 200 μL/min Ejection speed: 200 μL/min Injection volume: 1 μL | |
Minimum sample volume | 1 μL from 5 μL sample in 100 μL microvial, or 1 μL from 10 μL sample in 300 μL microvial. | Needle height offset has to be adapted to ensure that needle doesn’t touch vial bottom. Default needle height = 0 equates to 2 mm above the vial bottom. |
Control and data evaluation | Agilent OpenLab CDS MassHunter QQQ MassHunter TOF/QTOF Lab Advisor ICF for 3rd party SW control LC and CE Drivers | A.02.02 or above B.08.01 or above B.07.02 or above B.02.07 or above A.02.04 or above A.02.12 or above |
Local control | Agilent Instant Pilot (G4208A) | B.02.17 or above |
Communications | Controller-area network (CAN),Local Area Network (LAN) ERI: ready, start, stop and shut-down signals | |
Safety and maintenance | Extensive support for troubleshooting and maintenance is provided by the Instant Pilot, Agilent Lab Advisor, and the Chromatography Data System. Safety-related features are leak detection, safe leak handling, leak output signal for shutdown of pumping system, and low voltages in major maintenance areas. | |
GLP features | Early maintenance feedback (EMF) for continuous tracking of instrument usage with user-settable limits and feedback messages. Electronic records of maintenance and errors | |
Housing | All materials recyclable. | |
Metering device | Metering device in high pressure flow path |
Type | Specification | Comment |
Injection range | 0.1 – 20 μL in 0.1 μL increments (default) 0.1 – 40 μL in 0.1 μL increments if 40μL loop is installed 0.1 – 120 μL in 0.1 μL increments with 1290 Infinity large volume injection kit (hardware modification required) 0.1 – 100 μL in 0.1 μL (if 100 μL-loop and 100 μL-head is installed) | Up to 1500 μL with 1400 μL-multi-draw kit and 100 μL-analytical head up to 130 MPa (1300 bar, 18854 psi) up to 60 MPa (600 bar, 8702 psi) |
Precision | <0.25 % RSD of peak areas from 5 μL to 100 μL | Measured caffeine |
Pressure range | Up to 130 MPa (1300 bar, 18854 psi) | |
Sample viscosity range | 0.2 – 5 cp | |
Sample capacity | 132 x 2 mL vial (two trays default) 100 x 2 mL vial (two classic trays optional) 36 x 6 mL vials (two trays optional) | |
Carry over | <0.004 % (40 ppm) with needle wash | Using the following conditions: • ZORBAX Eclipse Plus C18, RRHD, 2.1 x 50 mm, 1.8 μm (959757-902) • Mobile Phase: • A: 0.1 % TFA in water • B: 0.1 % TFA in acetonitrile • Isocratic : % B=33 % • Flow rate: 0.5 mL/min • Column temperature: 50 °C • Wavelength detection: 257/4 nm, ref. wavelength 380/100 nm, 20 Hz • Injection volume: 1 μL • Sample: 1200 ng/μL Chlorhexidine for UV, (dissolved with mobile phase A), 1 μL injected and measured both on Agilent G7117B DAD • Wash solution: H2O with 0.1 % TFA (5 s) |
Injection cycle time | 18 s for draw speed 200 μL/min Ejection speed: 200 μL/min Injection volume: 1 μL | |
Minimum sample volume | 1 μL from 5 μL sample in 100 μL microvial, or 1 μL from 10 μL sample in 300 μL microvial. | Needle height offset has to be adapted to ensure that needle doesn’t touch vial bottom. Default needle height = 0 equates to 2 mm above the vial bottom. |
Control and data evaluation | Agilent OpenLab CDS MassHunter QQQ MassHunter TOF/QTOF Lab Advisor ICF for 3rd party SW control LC and CE Drivers | A.02.02 or above B.08.01 or above B.07.02 or above B.02.07 or above A.02.04 or above A.02.12 or above |
Local control | Agilent Instant Pilot (G4208A) | B.02.17 or above |
Communications | Controller-area network (CAN),Local Area Network (LAN) ERI: ready, start, stop and shut-down signals | |
Safety and maintenance | Extensive support for troubleshooting and maintenance is provided by the Instant Pilot, Agilent Lab Advisor, and the Chromatography Data System. Safety-related features are leak detection, safe leak handling, leak output signal for shutdown of pumping system, and low voltages in major maintenance areas. | |
GLP features | Early maintenance feedback (EMF) for continuous tracking of instrument usage with user-settable limits and feedback messages. Electronic records of maintenance and errors. | |
Housing | All materials recyclable. | |
Metering device | Metering device in high pressure flow path |
Type | Specification | Comments |
Weight | 15 kg (33 lbs) | |
Dimensions (height × width × depth) | 180 x 396 x 436 mm (7.1 x 15.6 x 17.2 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 70 W / 80 VA | |
Ambient operating temperature | 4–55 °C (39–131 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
(G7167B)
Type | Specification | Comments |
Weight | 22 kg (48.5 lbs) | w/o sample cooler |
Dimensions (height × width × depth) | 320 x 396 x 468 mm (12.6 x 15.6 x 18.4 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 180 VA, 180 W | |
Ambient operating temperature | 4 - 40 °C (39 - 104 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
Permitted solvents | Boiling point ≥56 °C Auto-ignition temperature ≥200 °C |
Multisampler (G5668A)
Type | Specification | Comments |
Weight | 22 kg (48.5 lbs) | w/o sample cooler |
Dimensions (height × width × depth) | 320 x 396 x 468 mm (12.6 x 15.6 x 18.4 inches) | |
Line voltage | 100 – 240 V~, ± 10 % | Wide-ranging capability |
Line frequency | 50 or 60 Hz, ± 5 % | |
Power consumption | 180 VA, 180 W | |
Ambient operating temperature | 4 - 40 °C (39 - 104 °F) | |
Ambient non-operating temperature | -40 – 70 °C (-40 – 158 °F) | |
Humidity | < 95 % r.h. at 40 °C (104 °F) | Non-condensing |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15092 ft) | For storing the module |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
Permitted solvents | Boiling point ≥56 °C Auto-ignition temperature ≥200 °C |
Type | Specification | Comment |
Injection range for Single-needle instruments | Default: 0.1 – 20 μL in 0.1 μL increments; optional: 40 μL or 100 μL (using 100 μL analytical head) | Up to 1300 bar using 40 μL (default) or optional 100 μL analytical head |
Pressure range up to 400 bar due to 900 μL analytical head | Pressure range up to 400 bar due to 900 μL analytical head | |
0.1 – 500 μL or 900 μL in 0.1 μL increments (using 900 μL analytical head) | Pressure range up to 1300 bar Multi-draw modus (Injection into needle-seat capillary | |
Injection range for Dual-needle instruments | Default: 0.1 – 20 μL in 0.1 μL increments; optional: 40 μL or 100 μL | Up to 1300 bar using 100 μL analytical head |
Up to 500 μL in 0.1 μL increments depending on installed loop size | Up to 1300 bar using 100 μL analytical head + Multi-load | |
Precision for Single-needle instruments | <0.15 % RSD or SD <10 nL, whatever is greater | Measured caffeine |
Precision for Dual-needle instruments | <0.2 % RSD or SD <10 nL, whatever is greater | Measured caffeine |
Pressure range | Up to 1300 bar (G7167B) | Max pressure for basic instrume |
Sample viscosity range | 0.2 – 5 cp | Max. 6144/1536 samples (384MTP/96) |
Sample capacity | 1H Drawer up to 8 drawers and 16 positions Shallow well plates (MTP) | 3072 samples, 432 vials (2 mL) |
2H Drawer up to 4 drawers and 8 positions MTP, deep well plates, vials, Eppendorf | 1536 samples, 60 vials (6 mL), 384 vials (1 mL), 216 vials (2 mL) | |
3H Drawer up to 2 drawers and 4 positions MTP, deep well plates, vials up to 6 mL, Eppendorf | Using standard Single-needle setup | |
Time between 2 injections is not mechanically limited, time delay depends on communication speed of software, OS or network connections | ||
Carry Over | <0.003 % (30 ppm) Multisampler Standard and Dual Needle <0.0009 % (9 ppm) Multisampler Multiwash | Using the following conditions: • Column: Agilent Pursuit XRs 3 C18, 2.0 x 50 mm • Mobile phase: • A: 0.1 % TFA in water • B: 0.1 % TFA in Acetonitrile • Isocratic : % B=40 % • Flow rate: 0.5 mL/min • Temperature: 25 °C • Wavelength: 257 nm • Sample: 1200 ng/μL Chlorhexidine (dissolved with mobile phase A), 1 μL injected and measured on G4212A DAD • Wash solution: H2O with 0.1 % TFA (3 s) |
Multiwash | Outer needle wash and seat backflush for carryover reduction with up to 3 different solvents | |
Control and data evaluation | Agilent Open Lab CDS | A.02.01 or above (A.02.02 supports Sample Entry UI) |
MassHunter QQQ | B.07.00 SP11 or above | |
MassHunter QTOF | B.05.01 SP31 or above | |
Lab Advisor | B.02.05 or above | |
ICF for 3rd party SW control | A.02.01 or above | |
LC and CE Drivers | A.02.10 or above | |
Local Control | Agilent Instant Pilot (G4208A) | B.02.17 or above (currently not supported/official release 2015) |
Communications | Controller-area network (CAN), Local Area Network (LAN) ERI: ready, start, stop and shut-down signals | |
Safety and maintenance | Extensive support for troubleshooting and maintenance is provided by the Instant Pilot, Agilent Lab Advisor, and the Chromatography Data System. Safety-related features are leak detection, safe leak handling, leak output signal for shutdown of pumping system, and low voltages in major maintenance areas. | |
GLP features | Early maintenance feedback (EMF) for continuous tracking of instrument usage with user-settable limits and feedback messages. Electronic records of maintenance and errors | |
Housing | All materials recyclable | |
Metering device | Metering device in high pressure flow path |
Table 4 Agilent 1260 Infinity Multisampler (G7167A) Performance Specifications
Type | Specification | Comment |
Injection range for Single-needle instruments | Default: 0.1 – 100 μL in 0.1 μL increments; optional: 20 μL or 40 μL (using optional 40 μL analytical head | Up to 600 bar using 100 μL (default) or optional 40 μL analytical head |
0.1 – 500 μL or 900 μL in 0.1 μL increments (using 900 μL analytical head) | Pressure range up to 400 bar due to 900 μL analytical head | |
0.1 – 120 μL in 0.1 μL increments with 1290 Infinity large volume injection kit (hardware modification required) G4216-68711 0.1 – 500 μL or 1500 μL in 0.1 μL increments with 100 μL upgrade kit (hardware modification required) G7167-68711 | Pressure range up to 600 bar Multi-draw modus (Injection into needle-seat capillary) | |
Injection range for Dual-needle instruments | Default: 0.1 – 100 μL in 0.1 μL increments; optional: 20 μL or 40 μL (using 100 μL analytical head) | Up to 600 bar using 100 μL analytical head |
Up to 900 μL in 0.1 μL increments depending on installed loop size | Up to 600 bar using 100 μL analytical head | |
Precision for Single-needle instruments | <0.15 % RSD or SD <10 nL, whatever is greater | Measured caffeine |
Precision for Dual-needle instruments | <0.2 % RSD or SD <10 nL, whatever is greater | Measured caffeine |
Pressure range | Up to 600 bar (G7167A) | Max pressure for basic instrument |
Sample viscosity range | 0.2 – 5 cp | |
Sample capacity | 1H Drawer up to 8 drawers and 16 positions Shallow well plates (MTP) | Max. 6144/1536 samples (384MTP/96) |
2H Drawer up to 4 drawers and 8 positions MTP, deep well plates, vials, Eppendorf | 3072 samples, 432 vials (2 mL) | |
3H Drawer up to 2 drawers and 4 positions MTP, deep well plates, vials up to 6 mL, Eppendorf | 1536 samples, 60 vials (6 mL), 384 vials (1 mL), 216 vials (2 mL) | |
Injection cycle time | <10 s using following standard conditions: Default draw speed: 100 μL/min | Using standard Single-needle setup |
Default eject speed: 400 μL/min Injection volume: 1 μL | Time between 2 injections is not mechanically limited, time delay depends on communication speed of software, OS or network connections | |
Carry Over | <0.003 % (30 ppm) Multisampler Standard and Dual Needle <0.0009 % (9 ppm) Multisampler Multiwash | Using the following conditions: • Column: Agilent Pursuit XRs 3 C18, 2.0 x 50 mm • Mobile phase: • A: 0.1 % TFA in water • B: 0.1 % TFA in Acetonitrile • Isocratic : % B=40 % • Flow rate: 0.5 mL/min • Temperature: 25 °C • Wavelength: 257 nm • Sample: 1200 ng/μL Chlorhexidine (dissolved with mobile phase A), 1 μL injected and measured on G4212A DAD • Wash solution: H2O with 0.1 % TFA (3 s) |
Multiwash | Outer needle wash and seat backflush for carryover reduction with up to 3 different solvents | |
Control and data evaluation | Agilent Open Lab CDS | A.02.01 or above (A.02.02 supports Sample Entry UI) |
MassHunter QQQ | B.07.00 SP11 or above | |
MassHunter QTOF | B.05.01 SP31 or above | |
Lab Advisor | B.02.05 or above | |
ICF for 3rd party SW control | A.02.01 or above | |
LC and CE Drivers | A.02.10 or above | |
Local Control | Agilent Instant Pilot (G4208A) | B.02.17 or above (currently not supported/official release 2015) |
Communications | Controller-area network (CAN), Local Area Network (LAN) ERI: ready, start, stop and shut-down signals | |
Safety and maintenance | Extensive support for troubleshooting and maintenance is provided by the Instant Pilot, Agilent Lab Advisor, and the Chromatography Data System. Safety-related features are leak detection, safe leak handling, leak output signal for shutdown of pumping system, and low voltages in major maintenance areas | |
GLP features | Early maintenance feedback (EMF) for continuous tracking of instrument usage with user-settable limits and feedback messages. Electronic records of maintenance and errors. | |
Housing | All materials recyclable | |
Metering device | Metering device in high pressure flow path |
Type | Specification | Comment |
Injection range | Default: 0.1 – 100 μL in 0.1 μL increments | Up to 600 bar using 100 μL |
Default: 0.1 – 250 μL or 1000 μL in 0.1 μL increments with Multidraw upgrade kit (Bio-inert) (G5667-68711 | Pressure range up to 400 bar Multi-draw mode (Injection into needle-seat capillary) | |
Precision | <0.15 % RSD or SD <10 nL, whatever is greater | Measured caffeine |
Pressure range | Up to 600 bar | Max pressure for basic instrument |
Sample viscosity range | 0.2 – 5 cp | |
Sample capacity | 1H Drawer up to 8 drawers and 16 positions Shallow well plates (MTP) | Max. 6144/1536 samples (384MTP/96) |
2H Drawer up to 4 drawers and 8 positions MTP, deep well plates, vials, Eppendorf | 3072 samples, 432 vials (2 mL) | |
3H Drawer up to 2 drawers and 4 positions MTP, deep well plates, vials up to 6 mL, Eppendorf | 1536 samples, 60 vials (6 mL), 384 vials (1 mL), 216 vials (2 mL) | |
Injection cycle time | <10 s using following standard conditions: Default draw speed: 100 μL/min | Using standard Single-needle setup |
Default eject speed: 400 μL/min Injection volume: 1 μL | Time between 2 injections is not mechanically limited, time delay depends on communication speed of software, OS or network connections | |
Carry Over | <0.003 % (30 ppm) Multisampler Standard <0.0009 % (9 ppm) Multisampler Multiwash | Using the following conditions: • Column: Agilent Pursuit XRs 3 C18, 2.0 x 50 mm • Mobile phase: • A: 0.1 % TFA in water • B: 0.1 % TFA in Acetonitrile • Isocratic : % B=40 % • Flow rate: 0.5 mL/min • Temperature: ambient • Wavelength: 257 nm • Sample: 1200 ng/μL Chlorhexidine (dissolved with mobile phase A), 1 μL injected and measured on G4212A DAD • Wash solution: H2O with 0.1 % TFA (3 s) |
Multiwash | Outer needle wash and seat backflush for carryover reduction with up to 3 different solvents | |
Materials in flow path | Titanium, gold, PTFE, PEEK, ceramic | Upstream of sample-introduction |
PEEK, ceramic | Downstream of sample-introduction | |
Control and data evaluation | Agilent Open Lab CDS | A.02.01 or above (A.02.02 supports Sample Entry UI) |
MassHunter QQQ | B.07.00 SP11 or above | |
MassHunter QTOF | B.05.01 SP31 or above | |
Lab Advisor | B.02.05 or above | |
ICF for 3rd party SW control | A.02.01 or above | |
LC and CE Drivers | A.02.10 or above | |
Local Control | Agilent Instant Pilot (G4208A) | B.02.17 or above (currently not supported/official release 2015) |
Communications | Controller-area network (CAN), Local Area Network (LAN), USB ERI: ready, start, stop and shut-down signals | |
Safety and maintenance | Extensive support for troubleshooting and maintenance is provided by the Instant Pilot, Agilent Lab Advisor, and the Chromatography Data System. Safety-related features are leak detection, safe leak handling, leak output signal for shutdown of pumping system, and low voltages in major maintenance areas. | |
GLP features | Early maintenance feedback (EMF) for continuous tracking of instrument usage with user-settable limits and feedback messages. Electronic records of maintenance and errors. | |
Housing | All materials recyclable. | |
Metering device | Metering device in high pressure flow path |
Table 5 Agilent 1260 Infinity II Bio-inert Multisampler (G5668A) Performance Specifications
Type | Specification | Comment |
Injection range | Default: 0.1 – 100 μL in 0.1 μL increments | Up to 600 bar using 100 μL |
Default: 0.1 – 250 μL or 1000 μL in 0.1 μL increments with Multidraw upgrade kit (Bio-inert) (G5667-68711 | Pressure range up to 400 bar Multi-draw mode (Injection into needle-seat capillary) | |
Precision | <0.15 % RSD or SD <10 nL, whatever is greater | Measured caffeine |
Pressure range | Up to 600 bar | Max pressure for basic instrument |
Sample viscosity range | 0.2 – 5 cp | |
Sample capacity | 1H Drawer up to 8 drawers and 16 positions Shallow well plates (MTP) | Max. 6144/1536 samples (384MTP/96) |
2H Drawer up to 4 drawers and 8 positions MTP, deep well plates, vials, Eppendorf | 3072 samples, 432 vials (2 mL) | |
3H Drawer up to 2 drawers and 4 positions MTP, deep well plates, vials up to 6 mL, Eppendorf | 1536 samples, 60 vials (6 mL), 384 vials (1 mL), 216 vials (2 mL) | |
Injection cycle time | <10 s using following standard conditions: Default draw speed: 100 μL/min | Using standard Single-needle setup |
Default eject speed: 400 μL/min Injection volume: 1 μL | Time between 2 injections is not mechanically limited, time delay depends on communication speed of software, OS or network connections | |
Carry Over | <0.003 % (30 ppm) Multisampler Standard <0.0009 % (9 ppm) Multisampler Multiwash | Using the following conditions: • Column: Agilent Pursuit XRs 3 C18, 2.0 x 50 mm • Mobile phase: • A: 0.1 % TFA in water • B: 0.1 % TFA in Acetonitrile • Isocratic : % B=40 % • Flow rate: 0.5 mL/min • Temperature: ambient • Wavelength: 257 nm • Sample: 1200 ng/μL Chlorhexidine (dissolved with mobile phase A), 1 μL injected and measured on G4212A DAD • Wash solution: H2O with 0.1 % TFA (3 s) |
Multiwash | Outer needle wash and seat backflush for carryover reduction with up to 3 different solvents | |
Materials in flow path | Titanium, gold, PTFE, PEEK, ceramic | Upstream of sample-introduction |
PEEK, ceramic | Downstream of sample-introduction | |
Control and data evaluation | Agilent Open Lab CDS | A.02.01 or above (A.02.02 supports Sample Entry UI) |
MassHunter QQQ | B.07.00 SP11 or above | |
MassHunter QTOF | B.05.01 SP31 or above | |
Lab Advisor | B.02.05 or above | |
ICF for 3rd party SW control | A.02.01 or above | |
LC and CE Drivers | A.02.10 or above | |
Local Control | Agilent Instant Pilot (G4208A) | B.02.17 or above (currently not supported/official release 2015) |
Communications | Controller-area network (CAN), Local Area Network (LAN), USB ERI: ready, start, stop and shut-down signals | |
Safety and maintenance | Extensive support for troubleshooting and maintenance is provided by the Instant Pilot, Agilent Lab Advisor, and the Chromatography Data System. Safety-related features are leak detection, safe leak handling, leak output signal for shutdown of pumping system, and low voltages in major maintenance areas. | |
GLP features | Early maintenance feedback (EMF) for continuous tracking of instrument usage with user-settable limits and feedback messages. Electronic records of maintenance and errors. | |
Housing | All materials recyclable. | |
Metering device | Metering device in high pressure flow path |
Table 6 Physical Specification of the Sample Cooler
Type | Specification | Comments |
Weight | < 6 kg | |
Dimensions (height × width × depth) | 205 mm x 340 mm x 370 mm | |
Refrigerant gas | HFC-134a (0.042 kg) | Ozone depletion potential (ODP) = 0 |
Supply voltage | 24 VDC (nominal) | |
Current | 10 A max. | |
Ambient operating temperature | 4 – 40 ° C (39.2 – 104 ° F) | |
Ambient non-operating temperature | -40 – 70 ° C (-20 – 158 ° F) | |
Operating altitude | Up to 3000 m (9842 ft) | |
Non-operating altitude | Up to 4600 m (15091 ft) | |
Safety standards: IEC, EN, CSA, UL | Installation category II, Pollution degree 2 | For indoor use only. |
ISM Classification | ISM Group 1 Class B | According to CISPR 11 |
Type | Specifications |
Operating principle | High performance, low-energy consumption micro-compressor based cooler with ozone-friendly HFC-134a coolant (42 g), user-upgradable. |
Temperature range | from 4 °C to 5 °C below ambient |
Temperature settable | from 4 – 40 °C in 1 ° increments |
Temperature accuracy (<25 °C, <50 % r.H.) | 2 °C to 6 °C at a setpoint of 4 °C |
3配置
NOS. | Parts No. | Description |
1 | G7110B 1260 Infinity II等度泵(大壓力 600 bar。包括等度泵 、色譜柱、連接毛細(xì)管、溶劑柜、溶劑瓶和 CAN 電纜。) | 1260 Infinity II Quaternary Pump |
2 | G7110B 001 液相工具包(液相色譜系統(tǒng)工具包。包括運行和維護(hù)安捷倫 1200 Infinity 系列液相色 譜系統(tǒng)所需要的工具。) | HPLC System Tool Kit, for Agilent 1260/1290 Infinity II LC |
3 | G7110B 032 主動閥套件 | Active Inlet Valve (AIV) |
4 | G7110B 030 泵頭密封墊清洗裝置 | Active Seal Wash |
5 | G1328C 1260 Infinity 手動進(jìn)樣器。包括 600 bar 的手動進(jìn)樣閥、20 μL樣品瓶和固定支架。 | 1260 Series Manual Injector. Includes Rheodyne 7725 manual injection valve, 20 ul sample loop and mounting stand. |
6 | G7111A 1260 Infinity II四元梯度泵含在線脫氣機(四元泵。大壓力 400 bar。包括內(nèi)置的四通道脫氣單元。包括四元泵、連接毛細(xì)管、溶劑柜和 CAN 電纜。) | 1260 Infinity II Quaternary Pump VL, maximum pressure 400bar. Includes quaternary pump, column, connecting capillaries, solvent cabinet, solvent bottles and CAN cable. |
7 | G7111A 001 液相工具包(液相色譜系統(tǒng)工具包。包括運行和維護(hù)安捷倫 1200 Infinity 系列液相色 譜系統(tǒng)所需要的工具。) | HPLC System Tool Kit, for Agilent 1260/1290 Infinity II LC |
8 | G7111A 032 主動閥套件 | Active Inlet Valve (AIV) |
9 | G7111A 030 泵頭密封墊清洗裝置 | Active Seal Wash |
10 | G7111B 1260 Infinity II四元梯度泵含在線脫氣機(1260 Infinity II 四元泵,大壓力 600 bar。包括四元泵 、連接毛細(xì)管、溶劑柜、溶劑瓶和 CAN 電纜。) | 1260 Infinity II Quaternary Pump VL, maximum pressure 600bar. Includes quaternary pump, column, connecting capillaries, solvent cabinet, solvent bottles and CAN cable. |
11 | G7111B 001 液相工具包(液相色譜系統(tǒng)工具包。包括運行和維護(hù)安捷倫 1200 Infinity 系列液相色 譜系統(tǒng)所需要的工具。) | HPLC System Tool Kit, for Agilent 1260/1290 Infinity II LC |
12 | G7111B 032 主動閥套件 | Active Inlet Valve (AIV) |
13 | G7111B 030 泵頭密封墊清洗裝置 | Active Seal Wash |
14 | G7111B 093 色譜柱 | Agilent Poroshell 120 EC-C18 4.6x100mm, 2.7um |
15 | G7122A 1260 Infi nity II 脫氣機 | 1260 Infi nity II Degasser 4 channels; up to 10 mL/min fl ow; 12mL internal volume per channel |
16 | G7129A 1260 Infinity II 樣品瓶進(jìn)樣器 (1260 Infinity II 樣品瓶進(jìn)樣器,耐壓達(dá) 600 bar。包括 100 μL 的計量裝置以及 100 μL 的樣品定量環(huán),帶集成進(jìn)樣針清洗口 。包括 2 個抽屜,每個抽屜可容納 66 個樣品瓶 (2 mL) | 1260 Infinity II Vialsampler for use up to 600 bar. Includes 100 uL metering device and a 100 uL sample loop plus integrated needle flush port. Includes 2 drawers each for 66 vials (2 mL). |
17 | G7167-60005 溫控器 | Infinity II Sample Cooler |
18 | G7129A 1260 ICC 063集成式柱溫箱 可容納 2 根色譜柱,加熱體積6 μL。) | 1260 Thermostatted Column Compartment |
19 | G7116A 1260 Infinity II 容量柱溫箱 可容納 2 根色譜柱,加熱體積 7 μL。) | 10 degrees below ambient to 85 °C; up to four 30 cm columns; up to four individual Infi nityLab Quick-Connect heat exchangers; optional valve drive for Infi nityLab Quick Change valve heads (up to 600 bar and up to 4-column selection without re-plumbing) |
20 | G7167A 1260 Infinity II Multisampler,耐壓達(dá) 600 bar,用于孔板和單個樣品容器。包括 2 個樣品抽屜、2 個 54 樣品瓶容器 、個進(jìn)樣針清洗口、100 μL 計量裝置和樣品定量環(huán)。 | 1260 Infinity II Multisampler |
21 | G7117C 1260 Infinity II 二極管陣列檢測器 HS。適用于靈敏度的快 速多波長光譜分析。數(shù)據(jù)采集速率達(dá) 120 Hz。用于流通池和燈的 RFID 標(biāo)簽。包括 10 mm 標(biāo)準(zhǔn)大光強卡套式流通池,體積1 μL | 5410是為快速離心少量樣品而設(shè)計的。外形精巧,運行時聲音極低,具備離心機所需性能:Short- spin 瞬時離心功能. |
22 | G7121A 1260 Infinity II 熒光檢測器(適用于可編程單波長檢測(激發(fā)和發(fā) 射),數(shù)據(jù)采集速率達(dá) 74 Hz。包括標(biāo)準(zhǔn)流通池,8μL) | 1260 Infinity II Variable Wavelength Detector |
23 | G7121B 1260 Infinity II 熒光檢測器(適用于多波長檢測,可在線采集 激發(fā)和發(fā)射光譜,采集速率達(dá) 148 Hz。包括標(biāo)準(zhǔn)流通池,8μL) | 1260 Infinity II Variable Wavelength Detector |
24 | G7162A 1260 Infinity II 示差折光檢測器。數(shù)據(jù)采集速率達(dá) 72 H z,配備集成式 8 μL 標(biāo)準(zhǔn)流通池 | 1260 Infinity II Refractive Index Detector |
25 | G4260B 蒸發(fā)光散射檢測器 | Agilent 1260 Infinity ELSD |
26 | ELSD模擬輸出電纜線 | 38x-ELSD Analogue Output Cable |
27 | M8301AA 工作站數(shù)據(jù)處理系統(tǒng) | OpenLAB CDS ChemStation Workstation |
28 | M8500AA 工作站采樣系統(tǒng) | OpenLAB CDS Inst. Driver for Agilent LC |
29 | M8410AA OpenLAB CDS 工作站軟件 | |
30 | M8410AA 001
液相色譜儀連接許可 |
|
31 | M8410AA 005 3D UV/DAD 連接許可 | |
32 | 5063-6591 手?jǐn)QPEEK接頭,1/16英寸,10/包 | PEEK finger-tight 1/16 in, 10PK |
33 | 0890-1763 PEEK管 | 1/16"od 0.007"id (0.18mm) 1.5m PEEK tbng |
34 | 8710-1930 塑料管線切割器 | Plastic and PEEK tubing cutter |
35 | 5182-0714 2mL廣口螺紋口玻璃瓶、透明,100個/包 | Vial,screw,2ml,clr,cert,100PK |
36 | 5182-0727 廣口,無隔墊螺紋口瓶蓋,用于2 mL 樣品瓶,100個/包 | Green color screw caps 100/PK |
37 | 5182-0731 PTFE/紅色硅橡膠乳白色隔墊,100/包 | Septa, PTFE/red silicone, 8.7mm 100/pk |
38 | 5063-6589 柱塞桿密封墊,石墨填充的PTFE(反相),(G1310A,G1311A,G1312A,G1376A,G2226A,1120,1220,G1310B,G1311B,G1312B,G1311C,G1312C,G4303A) | Plunger seal for 1100/1200 and 1050 2/PK |
39 | 01018-22707 過濾白頭,5/包 | PTFE Frits 5PK |
40 | 01018-60025 | Solvent inlet filter, stainless steel |
41 | 693970-902T 分析型液相色譜住,帶色譜柱 ID(InfinityLab Poroshell 120 色譜柱可在主流液相色譜系統(tǒng)壓力范圍內(nèi)實現(xiàn)穩(wěn)定的分離度分離,分析速度可比傳統(tǒng) 5µm 方法快 5 倍) | InfinityLab Poroshell 120 EC-C18,4.6×150 mm,4μm |
42 | 990967-902 XDB-C18色譜柱 (溫度上限:60℃, pH 圍:2.0-9.0) | XDB-C18 Analytical HPLC Col 4.6 x250 |
43 | 820950-925 保護(hù)柱芯,4/包 | Eclipse XDB-C18 4.6x12.5,5u Grd Car 4/PK |
44 | 820999-901 保護(hù)柱卡套 | High Perf. ZORBAX Guard Fittings Kit |
45 | SYS-LC-1260
硬件認(rèn)證 |
LC 1260 System |
46 | SYS-LC-1260 6N9
硬件IQ認(rèn)證 (安裝驗證) |
Enterprise Qualification IQ |
47 | SYS-LC-1260 6J9
硬件OQ認(rèn)證(操作驗證) |
Enterprise Qualification OQ 企業(yè)版操作認(rèn)證 |
48 | SYS-SW-OLAB-E
軟件認(rèn)證 |
OpenLAB CDS WorkStation |
49 | ||
50 | SYS-SW-OLAB-E 6N9
軟件IQ認(rèn)證(安裝驗證) |
Enterprise Qualification IQ |
51 | SYS-SW-OLAB-E 6J9
軟件OQ認(rèn)證(操作驗證) |
Enterprise Qualification OQ |
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